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October 23, 2021
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November 20, 2021
Published
March 1, 2022
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Abstract

Pemanfaatan batu kapur dari Pamekasan, Madura sebagai katalis heterogen pada reaksi pembuatan biodiesel dipelajari pada penelitian ini.  Batu kapur dikalsinasi pada suhu 900 ºC selama 3 jam untuk membentuk katalis CaO. Katalis CaO yang terbentuk dikarakterisasi menggunakan difraksi sinar-X (XRD), spektroskopi inframerah (FTIR) dan Scanning Electron Microscopy-Energy Dispersive X-Ray Analysis (SEM-EDX). Proses transesterifikasi dari minyak nyamplung dilakukan dengan rasio mol minyak terhadap methanol sebesar 1:16 pada temperatur 60 °C selama 1 jam dengan katalis CaO sebesar 4 % (w/w). Hasil analisis GC-MS diperoleh yield biodiesel sebesar 54% dengan konversi sebesar 49%.

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Febriana, I. D., Hamid, A., Jakfar, A., Abdullah, M., Rohmah, F., Purbaningtias, T. E., Rahmawati, Z., & Wijaya, S. D. (2022). Pemanfaatan Batu Kapur Madura sebagai Katalis dalam Pembuatan Bioedesel dari Minyak Nyamplung. Indonesian Journal of Chemical Analysis (IJCA), 5(1), 09–17. https://doi.org/10.20885/ijca.vol5.iss1.art2
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